HCID 86598914, compound → HCID 86598915, compound

Participants

Reaction Steps

To a solution of 2-tert-butyl 3-methyl (1R,3S,4S,6R)-6-azido-2-azabicyclo[2.2.1]heptane-2,3-dicarboxylate obtained in Example 29-2 (170 mg) in methanol (4 mL), was added 10% palladium on carbon (30 mg). The mixture was stirred under 1 atm of hydrogen for 1.5 hrs at room temperature. The resulting mixture was filtered through celite and washed with methanol. The filtrate and washings were evaporated in vacuo to give the target compound (155 mg).

Provenance & Evidence