HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 11757843, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 58818336 | HCID 58818336 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 11757843 | HCID 11757843 | — |
Reaction Steps
To a solution of 15 (312 mg, 0.46 mmol) in aqueous methanol was added a solution of 1.0M NaOH (1.5 eq). After 2 hours, reaction was complete by TLC. The solution was concentrated and purified by preparatory LC (C18, 100×20 mm I.D., 5 um). Product was isolated as a white amorphous solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07186746B2 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-2ffb9d4ab4fd45689e7db79ffe67bd68 |
| Source note | uspto-grants-2007_03 |