HCID 22291738, compound → HCID 22291719, compound

Participants

Reaction Steps

The title compound was synthesized from 0.355 g of the title compound of Step 1 and the title compound of Example 244 (0.32 g) by the same procedure used in Example 255. The title compound is a white solid (0.49 g, 87%). Its structure was confirmed by 1H NMR and LC/MS: 1H NMR (CD3CN): δ 2.18 (s, 6H), 2.57 (m, 2H), 2.85 (m, 4H), 3.00 (m, 4H), 3.26 (m, 2H), 5.88 (s, 1H), 6.94 (d, 1H), 7.27–7.38 (m, 5H), 7.47–7.62 (m, 3H), 7.69 (d, 1H, J=9 Hz), 9.40 (s, 1H). ESI mass spectrum for C28H27ClFN6O2S+: 565 (M+1).

Provenance & Evidence