HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20760150, compound → HCID 67378457, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20760150 | HCID 20760150 | — |
| Reactant | 4-{[(2R)-2,3-Dihydroxypropyloxy]phenyl}butylamine | HCID 67365743 | — |
| Product | HCID 67378457 | HCID 67378457 | 99% |
Reaction Steps
Compound 73 was prepared in a similar fashion to the synthesis of compound 70 starting from compound 72 (1.67 g, 4.5 mmol). Amine 73 (1.06 g, 99%) was isolated as a white solid. 1H NMR (300 MHz, DMSO-d6) δ 1.32 (m, 2H), 1.54 (m, 2H) 2.55 (m, 2H), 3.45 (m, 2H), 3.75 (m, 3H), 3.94 (m, 2H), 6.83 (d, 2H), 7.08 (d, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07189719B2 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-174884ba832d461790c76f5063f95ecc |
| Source note | uspto-grants-2007_03 |