HuagongsheHuagongshe Chemistry Print Report · For research reference only
56219-51-3 → HCID 69412675, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 56219-51-3 | HCID 10912216 | — |
| Reactant | Ethyl 4-(1H-indol-3-yl)piperidine-1-carboxylate | HCID 11380267 | — |
| Product | HCID 69412675 | HCID 69412675 | — |
Reaction Steps
This compound was prepared following the procedure described in example 13 (part B) at room temperature for 15 hours, starting with 2.2 g (8.1 mmol) of 4-(1H-indol-3-yl)-piperidine-1-carboxylic acid ethyl ester and 2.68 g (10 mmol) of 5-(3-bromo-propoxy)-benzo[1,3]dioxole. After standard work-up, 3.8 g (100% of yield) of the expected product was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07189741B2 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-063d5bca03b54568a280baf77be7013b |
| Source note | uspto-grants-2007_03 |