HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 2-(2-chloroethoxy)benzoate → HCID 10162976, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 2-(2-chloroethoxy)benzoate | HCID 9837283 | — |
| Reactant | HCID 17964389 | HCID 17964389 | — |
| Product | HCID 10162976 | HCID 10162976 | 22% |
Reaction Steps
This compound was prepared following the procedure described in Example 13 (part D) starting with 0.04 g (0.11 mmol) of 1-(2-[1,3]dioxolan-2-yl-ethyl)-6-fluoro-3-piperidin-4-yl-1H-indole and 0.03 g (0.15 mmol) of of 2-(2-chloro-ethoxy)-benzoic acid methyl ester. After purification over a Varian C18 column, 0.012 g (22% yield) were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07189741B2 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-47d2e9f2af4249db8f2966ff0d8f32f2 |
| Source note | uspto-grants-2007_03 |