Butanal → HCID 18440783, compound

HRID 457903Notes

Reaction equation

HRID 457903 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:10](=[CH:11][CH:12]=1)[CH:9]=[C:8]([C:13]1[N:14]=[C:15]([C:24]([CH3:28])([CH3:27])[CH2:25][NH2:26])[NH:16][C:17]=1[C:18]1[CH:23]=[CH:22][N:21]=[CH:20][CH:19]=1)[CH:7]=[CH:6]2.[CH:29](=O)[CH2:30][CH2:31][CH3:32]>>[CH2:29]([N:26]([CH2:4][CH2:3][CH2:12][CH3:11])[CH2:25][C:24]([C:15]1[NH:16][C:17]([C:18]2[CH:23]=[CH:22][N:21]=[CH:20][CH:19]=2)=[C:13]([C:8]2[CH:7]=[CH:6][C:5]3[C:10](=[CH:11][CH:12]=[C:3]([O:2][CH3:1])[CH:4]=3)[CH:9]=2)[N:14]=1)([CH3:28])[CH3:27])[CH2:30][CH2:31][CH3:32]

Participants

3

Reactant 2

HCID 261ButanalHCID 18440775HCID 18440775, compound

Product 1

HCID 18440783HCID 18440783, compoundYield 47%

Procedure

The title compound (12 mg, 47%) was prepared starting from the product of Example 2 and butyraldehyde using the method described in Example 25; MS(ES) m/e 485 [M+H]+.

Sources & evidence

ORD record
ord-903c9cc0cea844f998095661bee5747a
Source dataset
uspto-grants-2007_03
Patent number
US07189745B1

Reaction notes

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