HRID457927

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID821692

4-(Pyridin-2-yl)benzoic acid

C12H9NO2

结构：CON=C1C[C@@H](C(=O)OC)N(C(=O)OC(C)(C)C)C1

HCID58585478

未命名化合物

PRODUCTS

生成物

结构：CON=C1C[C@@H](C(=O)OC)N(C(=O)c2ccc(-c3ccccn3)cc2)C1

HCID131726287

未命名化合物

收率 45%

PROCEDURE

实验过程

Following the general method as outlined in Example 4 (Method B), starting from 1-tert-butyl 2-methyl (2S,4EZ)-4-(methoxyimino)-1,2-pyrrolidinedicarboxylate and 4-(2-pyridinyl)benzoic acid, the title compound was obtained, after flash-chromatography (eluent cyclohexane/ethyl acetate 8:2), as a mixture of two isomers in 45% yield (95% purity by HPLC).