HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11269582, compound → HCID 69431427, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11269582 | HCID 11269582 | — |
| Reactant | HCID 86584840 | HCID 86584840 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 69431427 | HCID 69431427 | — |
Reaction Steps
(2S,4R)-2-azidomethyl-4-tritylsulfanyl-pyrrolidine and benzyl chloroformate/N-ethyldiisopropylamine in CH2Cl2 (see cabamate synthesis, Method A)—followed by Staudinger reduction gave (2S,4R)-2-aminomethyl-4-tritylsulfanyl-pyrrolidine-1-carboxylic acid benzyl ester as white foam, MS: 509 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07189756B2 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-426f4d72a10d4daf90b0ccdff631b609 |
| Source note | uspto-grants-2007_03 |