HRID458341

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID98116

(3-Bromo-1-propen-1-yl)benzene

C9H9Br

结构：CS(=O)(=O)N1C[C@H](SC(c2ccccc2)(c2ccccc2)c2ccccc2)C[C@H]1CO

HCID69433309

未命名化合物

HCID131722655

未命名化合物

PRODUCTS

生成物

结构：CS(=O)(=O)N1C[C@H](S)C[C@H]1COCCCc1ccccc1

HCID86584849

未命名化合物

PROCEDURE

实验过程

(2S,4R)-(1-methanesulfonyl-4-tritylsulfanyl-pyrrolidin-2-yl)-methanol with 3-bromo-1-phenyl-1-propene, followed by hydrogenation (17 h) and TFA/triethylsilane deprotection (Method 3) gave (3R,5S)-1-methanesulfonyl-5-(3-phenyl-propoxymethyl)-pyrrolidine-3-thiol, MS: 329 (M).