HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69431418, compound → HCID 86584857, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69431418 | HCID 69431418 | — |
| Reactant | HCID 178418634 | HCID 178418634 | — |
| Product | HCID 86584857 | HCID 86584857 | — |
Reaction Steps
(3SR,5RS)-[5-Benzyloxymethyl-1-(naphthalene-2-sulfonyl)-piperidin-3-yl]-methanol (1.35 g) was reacted with thioacetic acid (see Mitsunobu reaction described in Example 17) to obtain thioacetic acid (3SR,5RS)-S-[5-benzyloxymethyl-1-(naphthalene-2-sulfonyl)-piperidin-3-ylmethyl] ester (0.92 g) as a syrup, MS: 484 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07189756B2 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-02c420f2d7464678ad9965f82d34b8e0 |
| Source note | uspto-grants-2007_03 |