HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Azide → 3-(4-Methoxyphenyl)propylazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | 3-(4-Methoxyphenyl)propyl methanesulfonate | HCID 11665938 | — |
| Product | 3-(4-Methoxyphenyl)propylazide | HCID 11715326 | 75% |
Reaction Steps
Azide 12 was prepared according to procedure C from 11 (8.8 g, 0.036 mol) and sodium azide (3 g, 0.045 mol) in 75% yield. 1H NMR (300 MHz, CDCl3) δ 1.90 (m, 2H), 2.65 (t, 2H), 3.28 (m, 2H), 3.80 (s, 3H), 6.85 (d, 2H), 7.10 (d, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07192959B2 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-0ae936a7e4e8412eb8fd55559cf08af4 |
| Source note | uspto-grants-2007_03 |