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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 458880Generated: October 30, 2026

Oxalyl chloride → HCID 57067848, compound

https://huagongshe.com/reaction/458880

Reaction equation

Participants

RoleNameHCIDCharge
ReactantOxalyl chlorideHCID 65578—
Reactant3-(3-Pyridinyl)-2-propenoic acidHCID 101984—
ReactantHCID 11623143HCID 11623143—
ProductHCID 57067848HCID 57067848—

Reaction Steps

Batch size: 6.1 g (41.0 mmol) 3-(3-pyridyl)-acrylic acid, 14.2 g (111.8 mmol) oxalyl chloride and 10.0 g (37.3 mmol) 4-(1,3-dioxo-1H,3H-benzo[de]isoquinolin-2-yl)-butylamine.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07192967B1
Source datasetuspto-grants-2007_03
ORD IDord-a98ff79d5b934af8815417ed3052d90c
Source noteuspto-grants-2007_03