HuagongsheHuagongshe Chemistry Print Report · For research reference only
Urea → 3-Phenylglutarimide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Urea | HCID 1176 | — |
| Reactant | 3-Phenylglutaric acid | HCID 77823 | — |
| Product | 3-Phenylglutarimide | HCID 101452 | — |
Reaction Steps
29.0 g (139 mmol) 3-phenylglutaric acid and 8.4 g (139 mmol) urea are stirred at 150° C. for 1.5 hours. After cooling, the reaction mixture is recrystallized from methanol: Yield 20.9 g (79%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07192967B1 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-51084e58044149e4a185e139ca8f0624 |
| Source note | uspto-grants-2007_03 |