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HRID458888

反应详情

EQUATION

反应方程式

HRID 458888 的结构方程式

REACTANTS

反应物

2
结构：COC(=O)C(O)(c1cccs1)c1cccs1
HCID11414137

Methyl 2,2-dithienylglycolate

C11H10O3S2

结构：O[C@@H]1CCN(CCCc2cccs2)C1
HCID11820472

未命名化合物

PRODUCTS

生成物

1
结构：O=C(O[C@@H]1CCN(CCCc2cccs2)C1)C(O)(c1cccs1)c1cccs1
HCID10048521

未命名化合物

收率 49.1%

PROCEDURE

实验过程

Prepared as described in Intermediate I-1 from 2-Hydroxy-2,2-dithien-2-ylacetic acid methyl ester and (3R)-1-(3-thien-2-ylpropyl)pyrrolidin-3-ol (Intermediate I-17). The yield was 0.83 g (49.1%) of the title product as an oil. A portion of this product was solidified by formation of the oxalate salt.

WORKUP

后处理

  1. customPrepared