Phenethyl bromide → HCID 69479834, compound

HRID 458900Notes

Reaction equation

HRID 458900 reaction equation
[NH:1]1[CH2:5][CH2:4][C@@H:3]([OH:6])[CH2:2]1.Br[CH2:8][CH2:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1>>[CH2:8]([N:1]1[CH2:5][CH2:4][C@@H:3]([OH:6])[CH2:2]1)[CH2:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1

Participants

3

Reactant 2

HCID 7666Phenethyl bromideHCID 2759337(R)-3-Pyrrolidinol

Product 1

HCID 69479834HCID 69479834, compoundYield 83.5%

Procedure

Prepared as in Intermediate I-15 from (3R)pyrrolidin-3-ol (commercially available) and (2-bromoethyl)benzene. The yield was 0.91 g (83.5%) of the title compound.

Sources & evidence

ORD record
ord-4ef63a15cc114c819377b056db2eb80f
Source dataset
uspto-grants-2007_03
Patent number
US07192978B2

Reaction notes

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