HRID459166

反应详情

EQUATION

反应方程式

HRID 459166 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of (2S)-3-{3-Allyl-4-[3-(4-phenoxy-phenoxy)-propoxy]-phenyl}-2-methoxy-propionic acid ethyl ester, from Example 148, Step B, was dissolved in ethanol and treated with H2 under balloon pressure. Filtered through a pad of celite and concentrated to dryness. The compound thus obtained was treated under, standard hydrolysis procedure C to give the title compound.

WORKUP

后处理

  1. additiontreated with H2 under balloon pressure
  2. filtrationFiltered through a pad of celite
  3. concentrationconcentrated to dryness
  4. customThe compound thus obtained
  5. additionwas treated under,
  6. customstandard hydrolysis procedure C