3-[4-(3-Bromo-propoxy)-3-methoxy-phenyl]-2-methoxy-propionic acid → HCID 18443630, compound
Reaction equation
Br[CH2:2][CH2:3][CH2:4][O:5][C:6]1[CH:11]=[CH:10][C:9]([CH2:12][CH:13]([O:17][CH3:18])[C:14]([OH:16])=[O:15])=[CH:8][C:7]=1[O:19][CH3:20].[CH:21]1[C:29]2[C:28]3[CH:30]=[CH:31][CH:32]=[CH:33][C:27]=3[O:26][C:25]=2[CH:24]=[C:23]([C:34]2[CH:39]=[CH:38][C:37]([OH:40])=[CH:36][CH:35]=2)[CH:22]=1>>[CH:21]1[C:29]2[C:28]3[CH:30]=[CH:31][CH:32]=[CH:33][C:27]=3[O:26][C:25]=2[CH:24]=[C:23]([C:34]2[CH:39]=[CH:38][C:37]([O:40][CH2:2][CH2:3][CH2:4][O:5][C:6]3[CH:11]=[CH:10][C:9]([CH2:12][CH:13]([O:17][CH3:18])[C:14]([OH:16])=[O:15])=[CH:8][C:7]=3[O:19][CH3:20])=[CH:36][CH:35]=2)[CH:22]=1Participants
3
Procedure
The title compound was prepared from 3-[4-(3-Bromo-propoxy)-3-methoxy-phenyl]-2-methoxy-propionic acid (Example 175, Step B) and 4-Dibenzofuran-3-yl-phenol following the Standard Procedure J. MS (ES) for C32H30O7 [M+NH4]+:544, [M+Na]+: 549.
Sources & evidence
- ORD record
- ord-3e391515dabc4523bda560231283a9bf
- Source dataset
- uspto-grants-2007_03
- Patent number
- US07192982B2
Reaction notes
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