HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(3-Bromopropoxy)1-phenoxybenzene → (S)-3-{4-[3-(4-phenoxy-phenoxy)-propoxy]-phenyl}-2-propoxy-propionic acid ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(3-Bromopropoxy)1-phenoxybenzene | HCID 11255243 | — |
| Reactant | (S)-3-(4-hydroxy-phenyl)-2-propoxy-propionic acid ethyl ester | HCID 58822755 | — |
| Product | (S)-3-{4-[3-(4-phenoxy-phenoxy)-propoxy]-phenyl}-2-propoxy-propionic acid ethyl ester | HCID 58822857 | — |
Reaction Steps
The title compound was prepared from (S)-3-(4-hydroxy-phenyl)-2-propoxy-propionic acid ethyl ester and 3-(4-phenoxy-phenoxy)-propyl bromide (Example 244) using the Standard Procedure L. The product was purified by column chromatography on silica gel using 9/1 Hexan/Ethyl acetate mixture as eluent to afford the title product. MS(ES) for C29H34O6 [M+NH4]+: 496.3
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07192982B2 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-03dfefd6370e4996b6a8ec3294fea298 |
| Source note | uspto-grants-2007_03 |