HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Hydroxide → HCID 10206217, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | HCID 69422492 | HCID 69422492 | — |
| Product | HCID 10206217 | HCID 10206217 | — |
Reaction Steps
The title compound was prepared from (S)-3-{4-[3-(4-benzoyl-phenoxy)-propoxy]-3-chloro-phenyl}-2-ethoxy-propionic acid methyl ester by the standard hydrolysis procedure C (LiOH). 1H-NMR (200.15 MHz, CDCl3): δ 7.82–7.72 (m, 4H), 7.56–7.43 (m, 3H), 7.07 (dd, 1H, J=8.8, 2.0), 6.97 (d, 2H, J=8.9), 6.86 (d, 2H, J=8.3), 4.31 (t, 2H, J=6.0), 4.21 (t, 2H, J=6.0), 4.10–4.02 (m, 1H), 3.66–3.44 (m, 2H), 3.10–2.87 (m, 2H), 2.33 (qn, 2H, J=6.2), 1.20 (t, 3H, J=7.0).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07192982B2 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-71dc1b4f73554fddbdbca81bd8ce4a4a |
| Source note | uspto-grants-2007_03 |