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HRID459277

反应详情

EQUATION

反应方程式

HRID 459277 反应方程式

REACTANTS

反应物

2
Methyl 4'-hydroxy[1,1'-biphenyl]-4-carboxylate 分子结构式
HCID1490289

Methyl 4'-hydroxy[1,1'-biphenyl]-4-carboxylate

C14H12O3

HCID 69424948 分子结构式
HCID69424948

未命名化合物

PRODUCTS

产物

1
HCID 58822569 分子结构式
HCID58822569

未命名化合物

PROCEDURE

实验过程

3-[4-(3-Bromo-propoxy)-3-methoxy-phenyl]-2-methoxy-propionic acid methyl ester (Step A) and 4′-hydroxy-biphenyl-4-carboxylic acid methyl ester (Example 197, Step A) were treated under Mitsunobu standard condition B. The crude was purified by chromatography on silica gel (hexanes/ethyl acetate 7:3) to afford the title compound.

WORKUP

后处理

  1. customThe crude was purified by chromatography on silica gel (hexanes/ethyl acetate 7:3)