HCID 69476650, compound → HCID 69478123, compound

HRID 459681Notes

Reaction equation

HRID 459681 reaction equation
C([O:8][CH2:9][C@@H:10]1[O:14][C:13](=[O:15])[C:12]([CH2:16][CH:17]([CH3:19])[CH3:18])=[CH:11]1)C1C=CC=CC=1>C(O)C>[OH:8][CH2:9][C@@H:10]1[O:14][C:13](=[O:15])[C:12]([CH2:16][CH:17]([CH3:19])[CH3:18])=[CH:11]1

Participants

3

Reactant 1

HCID 69476650HCID 69476650, compound

Product 1

HCID 69478123HCID 69478123, compoundYield 99%

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

2.3 g of [R]-5-benzyloxymethyl-3-isobutyl-2(5H)-furanone, 150 mg of PdOH/C in 50 ml of ethanol was stirred at RT over night under H2 atmosphere. Then the catalyst was filtered out and filtrate was evaporated to dryness to give the pure compound in yield of 99%.

Workup

  1. filtrationThen the catalyst was filtered out
  2. customfiltrate was evaporated to dryness
  3. customto give the pure compound in yield of 99%

Sources & evidence

ORD record
ord-e564ca57ba7e4059a3c6c0e00db128a6
Source dataset
uspto-grants-2007_03
Patent number
US07195719B1

Reaction notes

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