HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-hydroxy-3-(4-methoxyphenyl)benzyl Alcohol → HCID 22391344, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-hydroxy-3-(4-methoxyphenyl)benzyl Alcohol | HCID 68840635 | — |
| Catalyst | Manganese dioxide | HCID 14801 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 22391344 | HCID 22391344 | 108.8% |
Reaction Steps
A solution of 4-hydroxy-3-(4-methoxyphenyl)benzyl alcohol (5.54 g, 24 mmol) in acetone (250 mL) was treated with MnO2 and the mixture stirred for 3 days. The solid was filtered on diatomaceous earth and the filtrate was concentrated under reduced pressure to afford 5.96 g of title compound as a pale green oil, impure with manganese salts.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07196102B2 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-78aedaab8df1466bbb1ca93aa8c79a9b |
| Source note | uspto-grants-2007_03 |