HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Diaminopyridine → HCID 69410957, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Diaminopyridine | HCID 8861 | — |
| Reactant | tert-Butyl 2-formylpiperidine-1-carboxylate | HCID 10656219 | — |
| Product | HCID 69410957 | HCID 69410957 | — |
Reaction Steps
In a manner similar to that described in Preparation CD, 2-formyl-piperidine-1-carboxylic acid tert-butyl ester (360 mg, 1.69 mmol) was treated with 2,6-diaminopyridine (184 mg, 1.69 mmol) and stirred at RT to give a light brown oil. MS m/z: 307.3(M+H). Calc'd. for C16H26N4O2-306.21.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07196104B2 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-fbcd8bbb56c7421dbc80a3a1ac4c0888 |
| Source note | uspto-grants-2007_03 |