Methanol → HCID 59896206, compound

HRID 460335Notes

Reaction equation

HRID 460335 reaction equation
[NH2:1][CH2:2][CH2:3][S:4][CH2:5][C@@H:6]([C:8]([OH:10])=[O:9])[NH2:7].[CH3:11]O>>[NH2:1][CH2:2][CH2:3][S:4][CH2:5][C@@H:6]([C:8]([O:10][CH3:11])=[O:9])[NH2:7]

Participants

3

Reactant 2

HCID 887MethanolHCID 99558S-(2-Aminoethyl)-L-cysteine

Product 1

HCID 59896206HCID 59896206, compound

Procedure

A 10 g (50 mmol) sample of S-(2-aminoethyl)-L-cysteine was dissolved in 400 mL of methanol. Into this cooled solution was bubbled in anhydrous HCl for 30 minutes. After stirring at room temperature overnight, the solution was concentrated to afford 12.7 g of the title compound.

Workup

  1. customInto this cooled solution was bubbled in anhydrous HCl for 30 minutes
  2. concentrationthe solution was concentrated

Sources & evidence

ORD record
ord-4dd846f14cb74823b6db447a3bda5f9d
Source dataset
uspto-grants-2007_03
Patent number
US07196118B2

Reaction notes

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