3-Methoxypropylamine → HCID 10209864, compound
Reaction equation
CO[C:3](=[O:36])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][O:9][C:10]1[CH:11]=[CH:12][C:13]2[N:17]=[C:16]([S:18]([CH2:21][C:22]3[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=3)(=[O:20])=[O:19])[N:15]([C:28]3[CH:33]=[CH:32][C:31]([CH3:34])=[CH:30][CH:29]=3)[C:14]=2[CH:35]=1.[CH3:37][O:38][CH2:39][CH2:40][CH2:41][NH2:42]>>[CH3:37][O:38][CH2:39][CH2:40][CH2:41][NH:42][C:3](=[O:36])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][O:9][C:10]1[CH:11]=[CH:12][C:13]2[N:17]=[C:16]([S:18]([CH2:21][C:22]3[CH:23]=[CH:24][CH:25]=[CH:26][CH:27]=3)(=[O:19])=[O:20])[N:15]([C:28]3[CH:29]=[CH:30][C:31]([CH3:34])=[CH:32][CH:33]=3)[C:14]=2[CH:35]=1Participants
3
Procedure
100 mg of 6-[[1-(4-methylphenyl)-2-(phenylmethanesulfonyl)-1H-benzimidazol-6-yl]oxy]hexanoic acid methyl ester was reacted with 3-methoxypropylamine according to general operating instructions 4. 22 mg was obtained.
Workup
- custom22 mg was obtained
Sources & evidence
- ORD record
- ord-34833e9238cd4399a1112a43a12d2ed8
- Source dataset
- uspto-grants-2007_03
- Patent number
- US07196202B2
Reaction notes
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