HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
(S)-(+)-Glycidyl-4-nitrobenzoate → (s)-3-(4-Glycidyloxybenzo(b)furan-2-yl)-5-methyl-1,2,4-oxadiazole
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | (S)-(+)-Glycidyl-4-nitrobenzoate | HCID 10868995 | — |
| Edukt | 3-(4-Hydroxybenzo(b)furan-2-yl)-5-methyl-1,2,4-oxadiazole | HCID 135794306 | — |
| Produkt | (s)-3-(4-Glycidyloxybenzo(b)furan-2-yl)-5-methyl-1,2,4-oxadiazole | HCID 60078008 | 47,6% |
Reaktionsschritte
By the reactions in the same manner as in Starting Material Synthesis Example 1 using 3-(4-hydroxybenzo(b)furan-2-yl)-5-methyl-1,2,4-oxadiazole (0.75 g) and (S)-glycidyl nosylate (0.93 g), the title compound (0.45 g) was obtained as white crystals.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07196199B2 |
| Quelldatensatz | uspto-grants-2007_03 |
| ORD ID | ord-1e5cda0ba43649f7b283e917a93e6871 |
| Quellennotiz | uspto-grants-2007_03 |