化工社化工社 化学情報印刷レポート · 研究参考用
(S)-(+)-Glycidyl-4-nitrobenzoate → (s)-3-(7-Glycidyloxybenzo(b)furan-2-yl)-5-methyl-1,2,4-oxadiazole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | (S)-(+)-Glycidyl-4-nitrobenzoate | HCID 10868995 | — |
| 反応物 | 3-(7-Hydroxybenzo(b)furan-2-yl)-5-methyl-1,2,4-oxadiazole | HCID 22729084 | — |
| 生成物 | (s)-3-(7-Glycidyloxybenzo(b)furan-2-yl)-5-methyl-1,2,4-oxadiazole | HCID 60078028 | 90% |
反応手順
By the reactions in the same manner as in Starting Material Synthesis Example 1 using 3-(7-hydroxybenzo(b)furan-2-yl)-5-methyl-1,2,4-oxadiazole (1.5 g) and (S)-glycidyl nosylate (1.8 g), the title compound (1.7 g) was obtained as white crystals.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07196199B2 |
| 出典データセット | uspto-grants-2007_03 |
| ORD ID | ord-c6b521a5be9f4a2887e9c2643b940036 |
| 出典メモ | uspto-grants-2007_03 |