HuagongsheHuagongshe Chemistry Print Report · For research reference only
(S)-(+)-Glycidyl-4-nitrobenzoate → (S)-5-(4-glycidyloxybenzo(b)furan-2-yl)-2-methyl-1,3,4-oxadiazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (S)-(+)-Glycidyl-4-nitrobenzoate | HCID 10868995 | — |
| Reactant | 2-(5-Methyl-1,3,4-oxadiazol-2-yl)benzofuran-4-ol | HCID 135794324 | — |
| Product | (S)-5-(4-glycidyloxybenzo(b)furan-2-yl)-2-methyl-1,3,4-oxadiazole | HCID 60078060 | 28.3% |
Reaction Steps
By the reactions in the same manner as in Starting Material Synthesis Example 1 using 2-(4-hydroxybenzo(b)furan-2-yl)-5-methyl-1,3,4-oxadiazole (3.3 g) and (S)-glycidyl nosylate (3.7 g), the title compound (1.1 g) was obtained as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07196199B2 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-7fc530d19e9d44e488f1c2c7ab4a35be |
| Source note | uspto-grants-2007_03 |