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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 460582Generated: October 30, 2026

Triphenylphosphine → HCID 22728920, compound

https://huagongshe.com/reaction/460582

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriphenylphosphineHCID 11776—
Reactantethyl N-ethoxycarbonyliminocarbamateHCID 220568—
ReactantHCID 22729131HCID 22729131—
SolventTriethylamineHCID 8471—
ProductHCID 22728920HCID 2272892081.8%

Reaction Steps

By the reactions in the same manner as in Starting Material Synthesis Example 37 using N′-(4-methoxybenzo(b)furan-2-ylcarbonyl)trifluoroacetohydrazide (5.2 g), triethylamine (7.2 ml), triphenylphosphine (9.0 g) and diethyl azodicarboxylate (40% toluene solution, 6.2 ml), the title compound (4.0 g) was obtained as pale-yellow crystals.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07196199B2
Source datasetuspto-grants-2007_03
ORD IDord-69ef158838d745d7931de1aa21cddda2
Source noteuspto-grants-2007_03