HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → HCID 22728920, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | ethyl N-ethoxycarbonyliminocarbamate | HCID 220568 | — |
| Reactant | HCID 22729131 | HCID 22729131 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 22728920 | HCID 22728920 | 81.8% |
Reaction Steps
By the reactions in the same manner as in Starting Material Synthesis Example 37 using N′-(4-methoxybenzo(b)furan-2-ylcarbonyl)trifluoroacetohydrazide (5.2 g), triethylamine (7.2 ml), triphenylphosphine (9.0 g) and diethyl azodicarboxylate (40% toluene solution, 6.2 ml), the title compound (4.0 g) was obtained as pale-yellow crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07196199B2 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-69ef158838d745d7931de1aa21cddda2 |
| Source note | uspto-grants-2007_03 |