Boron tribromide → HCID 135794301, compound
Reaction equation
C[O:2][C:3]1[C:11]2[CH:10]=[C:9]([C:12]3[O:16][N:15]=[C:14]([CH3:17])[N:13]=3)[O:8][C:7]=2[CH:6]=[CH:5][CH:4]=1.B(Br)(Br)Br>>[OH:2][C:3]1[C:11]2[CH:10]=[C:9]([C:12]3[O:16][N:15]=[C:14]([CH3:17])[N:13]=3)[O:8][C:7]=2[CH:6]=[CH:5][CH:4]=1Participants
3
Procedure
By the reactions in the same manner as in Starting Material Synthesis Example 5 using 5-(4-methoxybenzo(b)furan-2-yl)-3-methyl-1,2,4-oxadiazole (0.98 g) and boron tribromide (3.1 ml), the title compound (0.72 g) was obtained as yellow crystals.
Sources & evidence
- ORD record
- ord-6c775ee4e28f4c8b8d5401bc568ba7f7
- Source dataset
- uspto-grants-2007_03
- Patent number
- US07196199B2
Reaction notes
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