Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetylglycine | HCID 10972 | — |
| Reactant | 4-Methoxybenzaldehyde | HCID 31244 | — |
| Reactant | Sodium Acetate | HCID 517045 | — |
| Solvent | Acetic Anhydride | HCID 7918 | — |
| Product | HCID 361416 | HCID 361416 | 52.8% |
Reaction Steps
Anisaldehyde (11.3 g), N-acetylglycine (9.8 g) and sodium acetate (8.2 g) were dissolved in acetic anhydride (200 ml) and the mixture was heated at 100° C. for 10 hr. After cooling, the precipitated yellow crystals were collected by filtration to give the title compound (9.52 g), melting point 151–153° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07196199B2 |
|---|
| Source dataset | uspto-grants-2007_03 |
|---|
| ORD ID | ord-023875ce2d2b4a1e973ba8e73dd78532 |
|---|
| Source note | uspto-grants-2007_03 |
|---|
