HuagongsheHuagongshe Chemistry Print Report · For research reference only
(S)-(+)-Glycidyl-4-nitrobenzoate → HCID 87858827, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (S)-(+)-Glycidyl-4-nitrobenzoate | HCID 10868995 | — |
| Reactant | HCID 22728960 | HCID 22728960 | — |
| Product | HCID 87858827 | HCID 87858827 | 79.6% |
Reaction Steps
By the reactions in the same manner as in Starting Material Synthesis Example 1 using 2-(7-hydroxybenzo(b)furan-2-yl)-5-methyloxazole (2.0 g) obtained in Starting Material Synthesis Example 65 and (S)-glycidyl nosylate (1.8 g), (S)-7-glycidyloxy-2-(5-methyloxazol-2-yl)benzo(b)furan (1.5 g) was obtained. Then, by the reactions in the same manner as in Example 1 using 4-(naphthalen-2-yl)piperidine (0.7 g), the title compound (0.26 g) was obtained, melting point 147–149° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07196199B2 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-80846dd805f24c3e9895ac042fa9bab1 |
| Source note | uspto-grants-2007_03 |