HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine hydrochloride → HCID 178515321, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine hydrochloride | HCID 11130 | — |
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | HCID 178515322 | HCID 178515322 | — |
| Product | HCID 178515321 | HCID 178515321 | — |
Reaction Steps
This material was then converted to the corresponding tetrazole 5-(4-benzyloxy-phenyl)-6-cyclohexyl-2-(1H-tetrazol-5-yl)-4H-pyrazolo[1,5-a]pyrimidin-7-one (551) via a previously described (sodium azide, triethylamine hydrochloride) experimental procedure (54% yield); LC-MS—calcd for C26H25N7O2 [M++H]+: 468.21, found: 468.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07196111B2 |
| Source dataset | uspto-grants-2007_03 |
| ORD ID | ord-0282b2b261f34d69b054209644744963 |
| Source note | uspto-grants-2007_03 |