Thionyl Chloride → HCID 53698365, compound

HRID 460752Notes

Reaction equation

HRID 460752 reaction equation
[CH2:1]([C:9]1[CH:19]=[CH:18][C:12]([CH:13]=[CH:14][C:15](O)=[O:16])=[CH:11][CH:10]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].S(Cl)([Cl:22])=O>>[CH2:1]([C:9]1[CH:19]=[CH:18][C:12]([CH:13]=[CH:14][C:15]([Cl:22])=[O:16])=[CH:11][CH:10]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 542659983-(4-Octylphenyl)prop-2-enoic acid

Product 1

HCID 53698365HCID 53698365, compound

Procedure

1.8 G. of p-n-octylcinnamic acid, prepared in a manner analogous to that described in Example 1, are boiled in 25 ml. of thionyl chloride for 30 minutes. The excess thionyl chloride is removed by distillation. The residue is taken up twice in absolute toluene, concentrated on a rotary evaporator and dried. There is thus obtained crude p-n-octylcinnamic acid chloride.

Workup

  1. customThe excess thionyl chloride is removed by distillation
  2. concentrationconcentrated on a rotary evaporator
  3. customdried

Sources & evidence

ORD record
ord-019bb038b60a4c4fbb3b562d0fd56bf3
Source dataset
uspto-grants-1977_12
Patent number
US04061587

Reaction notes

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