Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → 1-Phenyl-2-chloro-cyclohex-3-ene-carboxylic-acid-ethyl-ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | 1-Phenyl-2-acetoxy-cyclohex-3-ene-1-carboxylic acid-ethyl-ester | HCID 21394564 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 1-Phenyl-2-chloro-cyclohex-3-ene-carboxylic-acid-ethyl-ester | HCID 21394560 | — |
반응 단계
200 g of 1-phenyl-2-acetoxy-cyclohex-3-ene-1-carboxylic acid-ethyl-ester are dissolved in 1 liter of 96% ethanol. The solution is charged with 190 g of HCl gas and heated under reflux for 2 hrs. The solvent is removed and the residue directly fractionated in the vacuum. b.p.°,1 130° C. Yield: 169 g.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04061635 |
| 출처 데이터셋 | uspto-grants-1977_12 |
| ORD ID | ord-564c88fd42a544399a84ff288f33291c |
| 출처 메모 | uspto-grants-1977_12 |