HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N'-Dimethylthiourea → 4-(3,4-Dimethyl-5-sulfamoylphenyl)-3-methyl-2-methylimino-1,3-thiazolidine-4-ol-hydrobromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N'-Dimethylthiourea | HCID 2723631 | — |
| Reactant | 2-Bromo-3',4'-dimethyl-5'-sulfamoylacetophenone | HCID 21394783 | — |
| Product | 4-(3,4-Dimethyl-5-sulfamoylphenyl)-3-methyl-2-methylimino-1,3-thiazolidine-4-ol-hydrobromide | HCID 21394754 | — |
Reaction Steps
3.1 g of 2-bromo-3',4'-dimethyl-5'-sulfamoyl-acetophenon were reacted according to the method described in Example 6 with 1.1 g of 1,3-dimethyl-thiourea and the 4-(3,4-dimethyl-5-sulfamoylphenyl)-3-methyl-2-methylimino-1,3-thiazolidine-4-ol-hydrobromide was filtered off. M.p. 252°-255° C (decomposition).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04061647 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-e299688c5f68483b9780bbb34e181b73 |
| Source note | uspto-grants-1977_12 |