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HRID460843

反应详情

EQUATION

反应方程式

HRID 460843 的结构方程式

REACTANTS

反应物

2
结构：[Na+].[OH-]
HCID14798

Sodium Hydroxide

HNaO

结构：CCOC(=O)C(CC#CCCCC(=O)OC)(CCCC(COc1ccc(F)cc1)OC(C)=O)C(C)=O
HCID22759338

未命名化合物

PRODUCTS

生成物

1
结构：CC(=O)C(CC#CCCCC(=O)O)CCCC(O)COc1ccc(F)cc1
HCID22759232

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：CO
溶剂HCID887

Methanol

CH4O

结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

Methyl 8-acetyl-8-ethoxycarbonyl-12-acetoxy-13-(4-fluorophenoxy)-5-tridecynoate (40.00 g., 0.079 mole) is added to a solution of sodium hydroxide (18.96 g.; 0.474 mole) in water (132.7 ml.) and methanol (462.9 ml.). The resulting solution is allowed to stand for 191/2 hours at 55°.

WORKUP

后处理

  1. custom2 hours
  2. customat 55°