HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22759337, compound → HCID 22759307, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22759337 | HCID 22759337 | — |
| Reactant | HCID 22759338 | HCID 22759338 | — |
| Product | HCID 22759307 | HCID 22759307 | — |
Reaction Steps
The synthesis of this compound is carried out by the basic hydrolytic procedure described in Example 4, Step D except that an equivalent amount of ethyl 8-acetyl-8-ethoxycarbonyl-12-acetoxy-13-(4-fluorophenoxy)-10-tridecynoate is substituted for the methyl 8-acetyl-8-ethoxycarbonyl-12-acetoxy-13-(4-fluorophenoxy)-5-tridecynoate of Example 4, Step D. The product is purified by column chromatography on silica gel and is a light yellow viscous oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04061643 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-25a55e750b9d496dadc6e4aaf308e62a |
| Source note | uspto-grants-1977_12 |