1,10-Decanediol → Sulfamic acid, decamethylene ester

HRID 460878Notes

Reaction equation

HRID 460878 reaction equation
S(O[CH2:6][CH2:7][O:8][S:9](=[O:12])(=[O:11])[NH2:10])(=O)(=O)N.[CH2:13]([OH:24])[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20]CCO>>[S:9]([O:24][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:6][CH2:7][O:8][S:9](=[O:11])(=[O:12])[NH2:10])(=[O:11])(=[O:8])[NH2:10]

Participants

3

Reactant 2

HCID 371531,10-DecanediolHCID 148884Sulfamic acid, ethylene ester

Product 1

HCID 148885Sulfamic acid, decamethylene ester

Procedure

1,10-Bis-O-sulfamyl-1,10-decanediol is prepared in the same manner as 1,2-bis-O-sulfamyl-1,2-ethanediol in Example 1 except that 1,10-decanediol (67 g., 0.385 mol.) is employed as the alkanediol.

Sources & evidence

ORD record
ord-87efd3f8a46b4bc18c3fff6d5d0b8772
Source dataset
uspto-grants-1977_12
Patent number
US04061663

Reaction notes

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