HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzenamine, 4-methyl-, hydrochloride (1:1) → Azanium;4-ethenylbenzenesulfonate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzenamine, 4-methyl-, hydrochloride (1:1) | HCID 10891 | — |
| Edukt | Sodium 4-styrenesulfonate | HCID 3571582 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | Azanium;4-ethenylbenzenesulfonate | HCID 22660406 | — |
Reaktionsschritte
A 20.6 g sample of sodium p-styrenesulfonate was dissolved in 100 g of water. 14.4 g of p-toluidine hydrochloride was added to the resulting solution to precipitate a solid. The solid was filtered and was dissolved in 100 cc of aqueous solution containing 20 cc of 28.8% NH3 solution. As a result, ammonium p-styrenesulfonate was obtained in a conversion of 76%.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04061669 |
| Quelldatensatz | uspto-grants-1977_12 |
| ORD ID | ord-69d4eb1884e449f4a6f049c403e641db |
| Quellennotiz | uspto-grants-1977_12 |