HuagongsheHuagongshe Chemistry Print Report · For research reference only
beta-Aminobeta-ethoxyacrylic acid ethyl ester → HCID 20367254, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | beta-Aminobeta-ethoxyacrylic acid ethyl ester | HCID 278451 | — |
| Reactant | (3-chlorobenzyl)hydrazine | HCID 7219929 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20367254 | HCID 20367254 | 42% |
Reaction Steps
35 g (10% excess) of β-amino-β-ethoxyacrylic acid ethyl ester are introduced into 100 ml of ethanol. 32 g of 3-chlorobenzylhydrazine in 50 ml of ethanol are added while stirring. The mixture is worked up as above. 18.9 g of the compound identified above, as colorless felted needles of melting point 132°, are obtained. (Yield: 42% of theory)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04061653 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-4b3889ce8f9144939f4b92a692418706 |
| Source note | uspto-grants-1977_12 |