HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → HCID 20285675, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | HCID 20285690 | HCID 20285690 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 20285675 | HCID 20285675 | — |
Reaction Steps
A mixture of 25.4 g. (0.12 mol) of 3-chloromethyl-2,5-dichloro-4-methylthiophene, 34.6 g. (0.132 mol) of triphenylphosphine and 200 ml. of benzene was heated to the reflux overnight. The resulting beige solid was filtered to yield (2,5-dichloro-4-methyl-3-thenyl)-triphenylphosphonium chloride, m.p. 238°-240° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04061656 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-46ecad834d1d45d6955e4386ccc1e025 |
| Source note | uspto-grants-1977_12 |