HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53862496, compound → HCID 20313541, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53862496 | HCID 53862496 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20313541 | HCID 20313541 | — |
Reaction Steps
113.5 g (0.479 mol) of 2,4-dinitro-benzene-phosphonic acid dimethyl ester (1) dissolved in 1500 ml of methanol are hydrogenated at 35° C and 60 excess atmospheres in the presence of 25 g of Raney nickel.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04061697 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-5ba354766cb247749d50777f22cabe9f |
| Source note | uspto-grants-1977_12 |