alpha-Methyl-p-tridecylbenzylamine hydrochloride → 2-(alpha-Methyl-p-tridecylbenzylimino)hexahydroazepine hydrochloride

HRID 461025Notes

Reaction equation

HRID 461025 reaction equation
[ClH:1].[CH3:2][CH:3]([NH2:23])[C:4]1[CH:9]=[CH:8][C:7]([CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])=[CH:6][CH:5]=1.Cl.C[CH:26]([NH2:41])[C:27]1C=[CH:31][C:30](CCC2C=CC=CC=2)=[CH:29][CH:28]=1>>[ClH:1].[CH3:2][CH:3]([N:23]=[C:26]1[CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][NH:41]1)[C:4]1[CH:9]=[CH:8][C:7]([CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])=[CH:6][CH:5]=1

Participants

3

Reactant 2

HCID 13012102alpha-Methyl-p-tridecylbenzylamine hydrochlorideHCID 13012107alpha-Methyl-p-phenethylbenzylamine hydrochloride

Product 1

HCID 1784428352-(alpha-Methyl-p-tridecylbenzylimino)hexahydroazepine hydrochloride

Procedure

Following essentially the same procedure described in Example 7 but substituting α-methyl-p-tridecylbenzylamine hydrochloride for the α-methyl-p-phenethylbenzylamine hydrochloride above, results in the formation of 2-(α-methyl-p-tridecylbenzylimino)hexahydroazepine hydrochloride having a M.P. 183°-5° C.

Sources & evidence

ORD record
ord-38c3fded2c0248509f2b81d7f2b56632
Source dataset
uspto-grants-1977_12
Patent number
US04061746

Reaction notes

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