p-Dodecyloxy-alpha-methylbenzylamine hydrochloride → HCID 178443274, compound

HRID 461026Notes

Reaction equation

HRID 461026 reaction equation
[ClH:1].[CH2:2]([O:14][C:15]1[CH:23]=[CH:22][C:18]([CH:19]([NH2:21])[CH3:20])=[CH:17][CH:16]=1)[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH3:13].Cl.C[CH:26]([NH2:41])[C:27]1C=[CH:31][C:30](CCC2C=CC=CC=2)=[CH:29][CH:28]=1>>[ClH:1].[CH2:2]([O:14][C:15]1[CH:16]=[CH:17][C:18]([CH:19]([N:21]=[C:26]2[CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][NH:41]2)[CH3:20])=[CH:22][CH:23]=1)[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH3:13]

Participants

3

Reactant 2

HCID 13012104p-Dodecyloxy-alpha-methylbenzylamine hydrochlorideHCID 13012107alpha-Methyl-p-phenethylbenzylamine hydrochloride

Product 1

HCID 178443274HCID 178443274, compound

Procedure

Following essentially the same procedure described in Example 7 above and substituting p-dodecyloxy-α-methylbenzylamine hydrochloride for the α-methyl-p-phenyethylbenzylamine hydrochloride above, results in the formation of 2-(p-dodecyloxy-α-methylbenzylimino)hexahydroazepine hydrochloride having a M.P. of 186°-8° C (dec.).

Sources & evidence

ORD record
ord-38ac3a7b3d164440b70362beff807024
Source dataset
uspto-grants-1977_12
Patent number
US04061746

Reaction notes

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