alpha-Methyl-p-phenethylbenzylamine hydrochloride → N-[1-(4-phenoxyphenyl)ethyl]azepan-2-imine;hydrochloride

HRID 461028Notes

Reaction equation

HRID 461028 reaction equation
[ClH:1].[CH3:2][CH:3]([NH2:17])[C:4]1[CH:9]=[CH:8][C:7]([O:10][C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)=[CH:6][CH:5]=1.Cl.C[CH:20]([NH2:35])[C:21]1C=[CH:25][C:24](CCC2C=CC=CC=2)=[CH:23][CH:22]=1>>[ClH:1].[CH3:2][CH:3]([N:17]=[C:20]1[CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][NH:35]1)[C:4]1[CH:9]=[CH:8][C:7]([O:10][C:11]2[CH:12]=[CH:13][CH:14]=[CH:15][CH:16]=2)=[CH:6][CH:5]=1

Participants

3

Reactant 2

HCID 13012107alpha-Methyl-p-phenethylbenzylamine hydrochlorideHCID 130121121-(4-Phenoxyphenyl)ethan-1-amine hydrochloride

Product 1

HCID 135924608N-[1-(4-phenoxyphenyl)ethyl]azepan-2-imine;hydrochloride

Procedure

Following essentially the same procedure described in Example 7 above and substituting α-methyl-p-phenoxybenzylamine hydrochloride for the α-methyl-p-phenethylbenzylamine hydrochloride above, results in the formation of 2-(α-methyl-p-phenoxybenzylimino)hexahydroazepine hydrochloride having a M.P. of 210°-2° C., (dec.).

Sources & evidence

ORD record
ord-b4ee0369064b41e58c5cea28e2e56df5
Source dataset
uspto-grants-1977_12
Patent number
US04061746

Reaction notes

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