alpha-Methyl-p-phenethylbenzylamine hydrochloride → 2-[p-(2,2-Diphenylvinyl)-alpha-methylbenzylimino]hexahydroazepine hydrochloride

HRID 461029Notes

Reaction equation

HRID 461029 reaction equation
[ClH:1].[C:2]1([C:8]([C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)=[CH:9][C:10]2[CH:18]=[CH:17][C:13]([CH:14]([NH2:16])[CH3:15])=[CH:12][CH:11]=2)[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.Cl.C[CH:27]([NH2:42])[C:28]1C=[CH:32][C:31](CCC2C=CC=CC=2)=[CH:30][CH:29]=1>>[ClH:1].[C:19]1([C:8]([C:2]2[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=2)=[CH:9][C:10]2[CH:18]=[CH:17][C:13]([CH:14]([N:16]=[C:27]3[CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][NH:42]3)[CH3:15])=[CH:12][CH:11]=2)[CH:20]=[CH:21][CH:22]=[CH:23][CH:24]=1

Participants

3

Reactant 2

HCID 13012107alpha-Methyl-p-phenethylbenzylamine hydrochlorideHCID 13012109p-(2,2-Diphenylvinyl)-alpha-methylbenzylamine hydrochloride

Product 1

HCID 1784632922-[p-(2,2-Diphenylvinyl)-alpha-methylbenzylimino]hexahydroazepine hydrochloride

Procedure

Following essentially the same procedure described in Example 7 above and substituting p-(2,2-diphenylvinyl)-α-methylbenzylamine hydrochloride for the α-methyl-p-phenethylbenzylamine hydrochloride above, results in the formation of 2-[p-(2,2-diphenylvinyl)-α-methylbenzylimino]hexahydroazepine hydrochloride having a M.P. of 219°-21° C.

Sources & evidence

ORD record
ord-7e6ba2fb55774314bd06a6b8a122364d
Source dataset
uspto-grants-1977_12
Patent number
US04061746

Reaction notes

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