HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 4163384, compound → HCID 54270234, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 4163384 | HCID 4163384 | — |
| Solvent | Acetic Anhydride | HCID 7918 | — |
| Product | HCID 54270234 | HCID 54270234 | — |
Reaction Steps
1.0 g of 2,3-Bis(4-methoxyphenyl)-3-chloro-acrylaldoxime (3.14 mmoles) was refluxed for 2 hours in 25 ml of acetanhydride. After cooling, the mixture was poured onto water. The crystalline solid substance which had precipitated was suction-filtered and recrystallized from methanol. Melting point: 140° to 142° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04061772 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-dfea6051b49c45c2beb75072011364e4 |
| Source note | uspto-grants-1977_12 |