HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiourea → HCID 178437128, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiourea | HCID 2723790 | — |
| Reactant | 2-Methyl-3-hydroxy-4-chloromethyl-5-vinylpyridine | HCID 20263960 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178437128 | HCID 178437128 | — |
Reaction Steps
A mixture of 21.0 g. of 2-methyl-3-hydroxy-4-chloromethyl-5-vinylpyridine, 6.74 g. of thiourea, and 200 ml. of ethanol was refluxed 3 hours. The cooled mixture was filtered and the solids were washed with ether to give 2-methyl-3-hydroxy-4-isothioureidomethyl-5-vinylpyridine hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04061759 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-ce701da4fc8e41e4a52b32c6d0634039 |
| Source note | uspto-grants-1977_12 |